By R. Dupree, D. Holland (auth.), M. H. Lewis (eds.)
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Phys. (Paris), C8, 3. Gladden, L. , Carpenter, T. A. and Elliott, S. R. (1986a) Phi/os. , B53, L81. Gladden, L. , Carpenter, T. , Klinowski, J. and Elliott, S. R. (1986b)J. Magn. Reson. 66,93. , Harris, R. K. ' (1986)J. Chern. Soc. , 2247. Grimmer, A. , Hahnert, M. etal. (1984) Phys. Chern. Glasses, 25,105. Grimmer, A. R. and Muller, W. (1986) Monatsh. , 117,799. Grimmer, A. Rand Radeglia, R. (1984) Chern. Phys. , 106,263. John, C. , Alma, N. C. M. and Hays, G. R. (1983) Appl. , 6,341. , Kinsey, R.
S. (1984a) Philos. , 50, L13. Dupree, R, Holland, D. and Williams, D. S. (1985b) J. Phys. (Paris), C8, 119. Dupree, R, Holland, D. and Williams, D. S. (1985c) Phys. Chern. Glasses, 50. , Holland, D. and Williams, D. S. (1986a)J. Non-Cryst. Solids, 81,185. , Lewis, M. , Leng-Ward, G. and Williams, D. S. (1985d) J. Mater. Sci. , 4, 393. , Lewis, M. H. and Smith, M. E. (1986b) Phi/os. , 53A, L17. Dupree, R, Lewis, M. H. and Smith, M. E. (1988) J. Appl. Cryst. 21, 109. Dupree, Rand Pettifer, R F. (1984a) Nature (London), 308, 523.
The parent glass 35MgO· 20Al20 3·45B 20 3 produced three distinct Al resonances which were assigned to AI(OAI)4 at 58 ppm, AI(OB)4 at 29 ppm (based on the findings of Muller et al. (1983a) for the CaO-AI203-P20s system) and AI(OAI)6 at 1 ppm. The latter peak remained fairly constant in intensity over the composition range covered by the glass-forming region whereas the first two varied as the B 20 3 : Al 20 3 ratio changed, the second growing at the expense of the first as B20 3 is increased. On crystallization, the following changes to the spectrum are observed: (a) the AI(OAI)4 peak diminishes in size, (b) the AI(OB)4 peak moves to more positive chemical shift, (c) the AI(OAI)6 peak also moves more positive.